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Electron interferometry from voids in spinel

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Abstract

Voids in spinel can act as perfectly aligned double crystal interferometers. The electron interference patterns can be obtained by using a conventional TEM instrument operating in the convergent beam electron diffraction (CBED) mode. The study of the lattice fringes in the 2 beam case and in the case of [111] zone axis patterns (ZAPs), are reported. The (000) disc in CBED ZAPs shows a simple hexagonal pattern with an angular separation of ≈ 10-4 rad. The contrast within the (000) disc depends on the angle of convergence. A method for void size determination in the direction of the beam is presented. © 1984.
Original languageEnglish
Pages (from-to)233-239
Number of pages7
JournalUltramicroscopy
Volume13
Issue number3
DOIs
StatePublished - Jan 1 1984
Externally publishedYes

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